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Benzyl chloride

Benzyl chloride, or α-chlorotoluene, is an organic compound with the formula C6H5CH2Cl. This colorless liquid is a reactive organochlorine compound that is a widely used alkylating agent. Its strong alkylating tendency renders it hazardous.

Preparation
Benzyl chloride is prepared industrially by the gas-phase photochemical reaction of toluene with chlorine: : In this way, approximately 100,000 tonnes are produced annually. The reaction proceeds by the free radical process, involving the intermediacy of free chlorine atoms. Side products of the reaction include benzal chloride and benzotrichloride. Other methods of production exist, such as the Blanc chloromethylation of benzene. Benzyl chloride was first prepared from treatment of benzyl alcohol with hydrochloric acid. ==Uses and reactions==
Uses and reactions
Industrially, benzyl chloride is precursor to benzyl esters, which are used as plasticizers, flavorants, and perfumes. Quaternary ammonium salts, such as the benzalkonium chlorides used as surfactants, are produced by alkylation of tertiary amines with benzyl chloride. indoles and amines, and carbanions and enolates. Cyanide displaces chloride from benzyl chloride. The resulting benzyl cyanide is a precursor to phenylacetic acid, a precursor to pharmaceuticals and commercial fragrances. Phenols and alcohols are common oxygen-containing substrates, the product being benzyl ethers. In organic synthesis, these ethers serve as protecting groups. Debenzylation of such ethers can be achieved by hydrogenolysis using palladium on carbon. : Benzyl chloride undergoes hydrolysis to form benzyl alcohol: : When treated with aqueous sodium hydroxide, benzyl chloride converts to benzyl alcohol and dibenzyl ether, depending on conditions. Benzyl chloride also reacts readily with magnesium to produce a Grignard reagent. It is preferable over benzyl bromide for the preparation of this reagent, since the reaction of the bromide with magnesium tends to form the Wurtz coupling product 1,2-diphenylethane. Benzyl chloride is used to install benzyl groups on aromatic substrates. For example, when benzyl chloride is treated with benzene and aluminium trichloride under the conditions of Friedel-Crafts alkylation, it gives diphenylmethane. Heating benzyl chloride in the presence of aluminium trichloride gives poly(p-phenylene methylene): :{{chem2|n C6H5CH2Cl -> (C6H4CH2)_{n} + n HCl}} ==Safety and regulations==
Safety and regulations
Benzyl chloride is a lachrymator and has been used in chemical warfare. It is also very irritating to the skin. It is classified as an extremely hazardous substance in the United States as defined in Section 302 of the U.S. Emergency Planning and Community Right-to-Know Act (42 U.S.C. 11002), and is subject to strict reporting requirements by facilities which produce, store, or use it in significant quantities. Benzyl chloride may be used in the synthesis of amphetamine-class drugs, and for this reason, sales of benzyl chloride are monitored as a List II drug precursor chemical by the US Drug Enforcement Administration. ==See also==
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