MarketBis(trimethylsilyl)acetylene
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Bis(trimethylsilyl)acetylene

Bis(trimethylsilyl)acetylene (BTMSA) is an organosilicon compound with the formula Me3SiC≡CSiMe3 (Me = methyl). It is a crystalline solid that melts slightly above room temperature and is soluble in organic solvents. This compound is used as a surrogate for acetylene.

Reactions
BTMSA is used as a nucleophile in Friedel-Crafts type acylations and alkylations and a precursor to lithium trimethylsilylacetylide. The TMS groups can be removed with tetra-n-butylammonium fluoride (TBAF) and replaced with protons. BTMSA is also a useful reagent in cycloaddition reactions. Illustrating its versatility, BTMSA was used in a concise total synthesis of (±)-estrone. A key step in this synthesis was the formation of the steroidal skeleton, catalyzed by CpCo(CO)2. BTMSA also serves as a ligand in organometallic chemistry. For example, it forms stable adducts with metallocenes. : Cp2TiCl2 + Mg + Me3SiC≡CSiMe3 → Cp2Ti(η²-Me3SiC₂SiMe3) + MgCl2 == References ==
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