In October 1955
Geoffrey Wilkinson appointed him as a lecturer in inorganic chemistry at
Imperial College London. He was subsequently promoted to Senior Lecturer in 1963, Reader in 1964 and Professor in 1981. He was awarded an FRS in 1981. His research interests ranged widely over a number of topics in inorganic, organic and physical chemistry. Here we select just three areas which made a lasting contribution to chemistry. I. Measurement of
magnetic susceptibility. For
paramagnetic inorganic materials in particular, such measurements are often useful. In 1959, he devised a procedure, now called the Evans Method, in which an NMR tube containing the paramagnetic species is dissolved in water-
tert-butanol in the presence of a capillary of pure
tert-butanol. From the difference in positions of the 1H NMR peak of the hydroxyl peak of pure butanol and the same peak shifted by the paramagnetic substrate the susceptibility of the sample can be calculated. In 1967 he devised an ingenious modification of the classical
Gouy balance in which, instead of weighing the sample in a magnetic field, a small but powerful magnet was weighed against the static sample. This was further refined in 1974 by using two 6 g. strong magnets, each mounted on a torsion strip. The force that the static paramagnetic sample exerted on one magnet was balanced out by a current passed through a coil placed between the poles of the second magnet; by measurement of this current the magnetic susceptibility of the sample can be calculated. II
Nuclear magnetic resonance spectroscopy (NMR). In addition to his use of NMR to determine magnetic susceptibilities of species in solution (see above) he made wide use of the technique in the study of organometallic and coordination complexes. He also used the technique of double irradiation of organic compounds to establish the relative signs of coupling constants. III Inorganic chemistry. He made a number of studies on
organometallic and coordination complexes. An example of his ingenuity in this area is to show that divalent
lanthanides might show
Grignard-like behaviour, and to this end he found that samarium, europium and ytterbium formed such species and that they showed Grignard-type reactions. ==Personal life==