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Ubbelohde viscometer

An Ubbelohde type viscometer or suspended-level viscometer is a measuring instrument which uses a capillary based method of measuring viscosity. It is recommended for higher viscosity cellulosic polymer solutions. The advantage of this instrument is that the values obtained are independent of the total volume. The device was developed by the German chemist Leo Ubbelohde (1877-1964).

Determination of viscosity
The determination of viscosity is based on Poiseuille's law: : \frac{dV}{dt} = v \pi R^{2} = \frac{\pi R^{4}}{8 \eta} \left( \frac{- \Delta P}{\Delta x}\right) = \frac{\pi R^{4}}{8 \eta} \frac{ |\Delta P|}{L}, where t is the time it takes for a volume V to elute. The ratio \frac{dv}{dt} depends on R as the capillary radius, on the average applied pressure P, on its length L and on the dynamic viscosity η. The average pressure head is given by: :\Delta P = \rho g \Delta H \, with ρ the density of the liquid, g the Standard gravity and H the average head of the liquid. In this way the viscosity of a fluid can be determined. Usually the viscosity of a liquid is compared to a liquid with an analyte for example a polymer dissolved in it. The relative viscosity is given by: :\eta_r = \frac{\eta}{\eta_0} = \frac{t \rho}{t_0 \rho_0}, where t0 and ρ0 are the elution time and density of the pure liquid. When the solution is very diluted :\rho \simeq \rho_0 \, the so-called specific viscosity becomes: :\eta_{sp} = \eta_r - 1 = \frac{t - t_0}{t_0}. \, This specific viscosity is related to the concentration of the analyte through the Intrinsic viscosity [η] by the power series: :\eta_{sp} = [\eta] c + k [\eta]^2 c^2 + \cdots\, or :\frac{\eta_{sp}}{c} = [\eta] + k[\eta]^2 c + \cdots,\, where \frac{\eta_{sp}}{c} is called the viscosity number. The intrinsic viscosity can be determined experimentally by measuring the viscosity number as function of concentration as the Y-axis intercept. == References ==
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