Achieving high pressure and pressure calibration methods Mao is one of the most prolific users of the
diamond anvil cell for research at high pressures. Although at the time the claim was controversial, his work with Peter M. Bell is now generally accepted as being the first verified
static pressure in excess of 1 Megabar. Mao and colleagues first calibrated
ruby fluorescence pressure scale to 80 GPa and this method has been widely used in almost every diamond anvil cell experiments. This work has been cited by 3921 times as of Jan 15, 2022, according to google scholar. In 2018, 400 GPa was achieved by his team and a detailed description of pressure loading and distribution, gasket thickness variation, and diamond anvil deformation was reported.
Towards metallic hydrogen Mao is a pioneer in experimentally exploring the possible
metallic hydrogen phase under high pressure. His work on solid hydrogen starts in 1988, where he reported
single-crystal structure of hydrogen up to 26.5 GPa. He later published a review paper on transitions in solid hydrogen in 1994. In 1996, his team's work suggested a more compressible solid hydrogen than previously thought. More recently in 2019, his team published results on single crystal diffraction of the lightest material in the world,
hydrogen, up to 254 GPa and revealed isostructural electronic transitions in solid hydrogen at around 220 GPa. ===
Superconductivity === In 1987, Mao and a colleague at the Geophysical Laboratory,
Robert Hazen, identified the composition and structure of the first
high-temperature superconductor to have a
critical temperature above the boiling point of
liquid nitrogen.
Iron peroxide in Earth's interior Mao discovered formation of FeO2Hx from
goethite FeOOH or from iron-water reaction under Earth's lower mantle conditions. The novel FeO2Hx phase processes a pyrite structure. Since this phase can contain varied amount of
hydrogen, it would have important implications for the
deep water cycle. ==Honors and awards==