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Efflorescence

In chemistry, efflorescence is the migration of a salt to the surface of a porous material, where it forms a coating. The essential process involves the dissolving of an internally held salt in water or occasionally, in another solvent. The water, with the salt now held in solution, migrates to the surface, then evaporates, leaving a coating of the salt.

Examples
• A 5 molar concentration aqueous droplet of NaCl will spontaneously crystallize at 45% relative humidity (298 K) to form an NaCl cube by the mechanism of homogeneous nucleation. The original water is released to the gas phase. • Gypsum (CaSO4.2H2O) is a hydrate solid that, in a sufficiently dry environment, will give up its water to the gas phase and form anhydrite (CaSO4). • Copper(II) sulfate (bluestone) (CuSO4.5H2O) is a blue crystalline solid that when exposed to air, slowly loses water of crystallization from its surface to form a white layer of anhydrous copper(II) sulfate. • Sodium carbonate decahydrate (Na2CO3.10H2O) will lose water when exposed to air. ==Masonry==
Masonry
Primary efflorescence Primary efflorescence is named such, as it typically occurs during the initial cure of a cementitious product. It often occurs on masonry construction, particularly brick, as well as some firestop mortars, when water moving through a wall or other structure, or water being driven out as a result of the heat of hydration as cement stone is being formed, brings salts to the surface that are not commonly bound as part of the cement stone. As the water evaporates, it leaves the salt behind, which forms a white, fluffy deposit, that can normally be brushed off. The resulting white deposits are referred to as "efflorescence" in this instance. In this context efflorescence is sometimes referred to as "saltpetering." Since primary efflorescence brings out salts that are not ordinarily part of the cement stone, it is not a structural, but, rather, an aesthetic concern. For controlling primary efflorescence, formulations containing liquid fatty acid mixtures (e.g., oleic acid and linoleic acid) have commonly been used. The oily liquid admixture is introduced into the batch mix at an early stage by coating onto the sand particles prior to the introduction of any mix water, so that the oily admixture is distributed uniformly throughout the concrete batch mix. Protecting against efflorescence It is possible to protect porous building materials such as brick, tiles, and concrete against efflorescence by treating the material with an impregnating, hydro-phobic sealer. This is a sealer that repels water and will penetrate deeply enough into the material to keep water and dissolved salts well away from the surface. However, in climates where freezing is a concern, such a sealer may lead to damage from freeze/thaw cycles. And while it will help to protect against efflorescence, it cannot permanently prevent the problem. Common rebar protective measures include the use of epoxy coating. Certain cement types are less resistant to chlorides than others. The choice of cement, therefore, can have a large effect upon the concrete's reaction to chlorides. Today's water repellents help create a vapor permeable barrier; liquid water, especially from wind driven rains, will stay out of the brick and masonry. Water vapor from the interior of the building, or from the underside of pavers can escape. This will reduce efflorescence, spalling and scaling that can occur from water being trapped inside the brick substrate and freezing during cold weather. Years ago, the water repellents trapped moisture in the masonry wall creating more problems than they solved. Condensation in areas that experienced the four seasons were much more problematic than their counterparts. Image gallery Image:Ausblühungen.JPG|Primary efflorescence on a brick wall in Germany. Image:K10 primary efflorescence.jpg|Primary efflorescence on a firestop mortar at Mississauga Civic Centre in Mississauga, Ontario City Hall. Image:Efflorescence.JPG|Substantial primary efflorescence on a building in Denver, Colorado. Image:Secondary efflorescence 1 of 2.jpg|Secondary efflorescence - dissolving the cement stone and attacking rebar Image:Secondary efflorescence 2 of 2.jpg|Secondary efflorescence Image:Concrete stalactite.jpg|Concrete derived secondary deposit of calcium carbonate creating calthemite stalactites, which can be mistakenly confused with efflorescence. ==See also==
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